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Grant: Research Tools and Instruments - Category 1 (<$150,000)

University of British Columbia

$150,000.00

Real-time back-reflection Laue Camera System for single-crystal alignment and characterization

EF 2010-11

Résumé
X-ray diffraction, with its ability of providing complete information on the crystal structure of solids, is one of the most fundamental and widespread tools in materials science and materials processing. To this end, and among the many modern applications, two standard techniques are available for single crystals: - Single-crystal diffractometry. This is oldest and yet most precise method for the complete determination of the structure of single crystals (including atomic positions, bond lengths, and bond angles). - Laue diffractometry. Although not well suited for determining a yet unknown crystal structure, especially for complex materials, it provides a great deal of information in a very short exposure. Laue allows the fast characterization, alignment, and processing of already known single crystals, for which purposes the use of single-crystal diffractometry is too time consuming and thus inefficient. At UBC no Laue diffractometry facility is currently available in any of the departments on campus. This has become a critical impediment in much of the ongoing materials research work relying on 'well aligned' single crystals either for advanced-spectroscopy experiments or for further materials processing, such as the growth of novel oxides heterostructures and quantum materials. We are here proposing the purchase of a state-of-the-art real-time Laue camera system. Based on a position sensitive x-ray proportional counter connected to a custom computer system, and joystick controlled motorized orientation stages, this instrument allows orienting a single crystal extremely rapidly, while observing the corresponding Laue pattern evolve truly in real time. This also represents the ideal replacement for the Polaroid XR-7 back-reflection cassette of the previous generation Laue cameras, for which films will eventually no longer be available since Polaroid ceased production in 2008.
Programme
Research Tools and Instruments - Category 1 (<$150,000)
Emplacement
British Columbia, Canada
Type de bénéficiaire
Academia
Type
Grant
Source
NSERC's Awards Data

Tel que publié

Application id
406595-2011
Name nom
Damascelli, Andrea
Department département
Physics and Astronomy
Organization id
2
Institution établissement
University of British Columbia
Province en
British Columbia
Province fr
Colombie-Britannique
Country en
CANADA
Country fr
CANADA
Fiscal year exercice financier
2010
Competition year année de concours
2011
Award amount
150000
Program id
EQPEQ
Program name en
Research Tools and Instruments - Category 1 (<$150,000)
Program name fr
Outils et instruments de recherche - catégorie 1 (<150 000$)
Group en
Discovery grants programs
Group fr
Programmes de subventions à la découverte
Committee code
1505
Committee name en
Physics
Committee name fr
Physique
Area of application code
1208
Area of application group en
Advancement of knowledge
Area of application group fr
Avancement des connaissances
Area of application en
Materials sciences
Area of application fr
Sciences des matériaux
Research subject code
2001
Research subject group en
Materials science and technology
Research subject group fr
Science et technologie des matériaux
Research subject en
Materials structure, properties and testing
Research subject fr
Structure, propriétés et essais des matériaux
Partie
1
Nb partie
1
Application title
Real-time back-reflection Laue Camera System for single-crystal alignment and characterization
Keyword
NSERC
Application summary
X-ray diffraction, with its ability of providing complete information on the crystal structure of solids, is one of the most fundamental and widespread tools in materials science and materials processing. To this end, and among the many modern applications, two standard techniques are available for single crystals: - Single-crystal diffractometry. This is oldest and yet most precise method for the complete determination of the structure of single crystals (including atomic positions, bond lengths, and bond angles). - Laue diffractometry. Although not well suited for determining a yet unknown crystal structure, especially for complex materials, it provides a great deal of information in a very short exposure. Laue allows the fast characterization, alignment, and processing of already known single crystals, for which purposes the use of single-crystal diffractometry is too time consuming and thus inefficient. At UBC no Laue diffractometry facility is currently available in any of the departments on campus. This has become a critical impediment in much of the ongoing materials research work relying on 'well aligned' single crystals either for advanced-spectroscopy experiments or for further materials processing, such as the growth of novel oxides heterostructures and quantum materials. We are here proposing the purchase of a state-of-the-art real-time Laue camera system. Based on a position sensitive x-ray proportional counter connected to a custom computer system, and joystick controlled motorized orientation stages, this instrument allows orienting a single crystal extremely rapidly, while observing the corresponding Laue pattern evolve truly in real time. This also represents the ideal replacement for the Polaroid XR-7 back-reflection cassette of the previous generation Laue cameras, for which films will eventually no longer be available since Polaroid ceased production in 2008.